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Di-n-butyl Peroxydicarbonate (CAS 16215-49-9): Technical Guide for Low-Temperature Polymerization & Safety Management​

· Organic Peroxide,Perodox

Di-n-butyl Peroxydicarbonate (BPC, CAS 16215-49-9), a ​​high-efficiency low-temperature initiator​​, is critical for optimizing vinyl chloride polymerization and specialty resin synthesis. With the molecular formula ​​C₁₀H₁₈O₆​​ and molecular weight of ​​234.2 g/mol​​, this organic peroxide enables precise molecular weight control while minimizing defects like "fish eyes" in PVC, LDPE, and acrylic production . Its theoretical active oxygen content of ​​6.83%​​ and decomposition temperature as low as ​​49°C​​ make it indispensable for energy-efficient industrial processes .

Technical Specifications & Physicochemical Properties

​​Parameter​​

​​Value​​

​Physical State​

Clear liquid (50% solution in inert solvents)

​Active Oxygen Content​

3.41% (typical commercial grade)

​Theoretical Active Oxygen​

6.83%

​UN Transport Class​

UN 3115 (Type E organic peroxide)

​Critical Safety Parameters​​:

- ​​Self-Accelerating Decomposition Temperature (SADT)​​: 5°C

- ​​Half-Life (t₁/₂)​​: 10h at 49°C, 1h at 65°C, 0.1h at 83°C

- ​​Storage Stability​​: ≤3 months below -15°C; ​​emergency threshold​​: -5°C

Decomposition Byproducts​​: Carbon dioxide + n-butanol — recyclable in solvent recovery systems .


Industrial Applications Driving Demand​

​1. PVC Suspension Polymerization​

As a ​​primary low-temperature initiator​​, BPC enables:

  • ​Energy Savings​​: Operates at 45–60°C (vs. 70–90°C for traditional peroxides), reducing cooling costs by 30% .
  • ​Defect Reduction​​: ≤25% fewer "fish eyes" in rigid PVC pipes by optimizing nucleation kinetics .
  • ​Co-polymer Compatibility​​: Efficient initiation for vinyl chloride/acrylate blends in adhesive resins .

​2. Specialty Polymer Synthesis​

  • ​Acrylic Casting​​: Initiates methyl methacrylate (MMA) polymerization at 50°C with >95% monomer conversion .
  • ​Expandable Polystyrene (EPS)​​: Controls cell structure uniformity in foam products .

Safety Protocols: Non-Negotiable Handling Rules​​

BPC’s ​​extremely low SADT (5°C)​​ mandates stringent protocols:

Storage​​: ≤-15°C in sealed containers; isolate from acids, metals, and reducing agents .

​​PPE Requirements​​: Butyl rubber gloves + full-face shields during handling .

​​Emergency Response​​:

​​Fire​​: Use alcohol-resistant foam — ​​water jets trigger explosive decomposition​​ .

​​Spills​​: Absorb with inert materials (vermiculite/sand); store in ventilated plastic containers .

️ ​​Regulatory Compliance​​:

GHS Classification: H242 (Heating may cause fire) .

  • Transport Restrictions: Prohibited in air transport; requires temperature-controlled vehicles (-20°C) for road shipping .

Future Innovations & Sustainability Trends​​

​​Microencapsulation Technology​​: Silica-based coatings to stabilize BPC at 0°C (pilot trials, 2026) .

​​Bio-Solvent Systems​​: Replacing phthalate carriers with soybean oil derivatives to reduce toxicity .

​​AI-Driven Storage Sensors​​: Real-time temperature/pressure monitoring during logistics .

​​Di-n-butyl Peroxydicarbonate (CAS 16215-49-9)​​ remains pivotal for sustainable polymer manufacturing, balancing low-temperature reactivity with evolving safety standards.